GCMS analysis results for sample AE05896, March 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5896.D Vial: 24 Acq On : 22 Mar 2002 11:57 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 5-Oxazolecarboxamide, 2-phenyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.23 ug/1 78884 Phenanthrene-dl0 25.67

Hit# of 5 Tentrative ID MW MolForm ■ CAS# Qual

1 5-Oxazolecarb^amide, 2-phenyl- 188 C10H8N2O2 039819-42-6 47 2 Anthracene-dTO- 188 C14D10 001719-06-8 40 3 Antipyrine / 188 C11H12N2O 000060-80-0 40 4 Phenanthrene-dlO 188 C14D10 001517-22-2 38 Abundance"...... .. . ... .... S"can“226l"(25.799 mfn)?5896.D {-y m/z 188.10 Too.00% 1 i8

5000

80 94 i 25.40 25.60 25.80 26.00 26.20 42 52 66 I I 132 146 ''' I''' ''i I' m/z 94.05 14.39% rn/z-->______ 40__ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19812: 5-dxazoiecarboxamide.2-phenyi- 116 144 1$8

5000 __________________ 89 25.40 25'60 25.80 26.00 26.20 63 m/z 189.10 13.85% 105 X-T TtT-r I I''' ' I m/2-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957; Anthracene-dlO- 188 I 2540 25,60 25^ 26^00 26.20 5000 m/z 184.10 13.67%

80 94 160 DO

Tn/z->_____ 40 50 60 70 80 90 100 UI 120__130 140 150 160 170 J 80 J 90 Abundance #69176: Antipyrine 1 18 25.40 25.60 25.80 26.00 26.20 m/z 8 . 05 -11.78% 96 5000 77 56 105 159 ip I'«'' I " ' I'l' " ' I " '' I m/2-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25-80 26.00 26.20

5896.D GCMS0308.M Mon Mar 25 14:26:07 2002 Page 1

NYC-WTC_000059752