GCMS calibration data for Method 508, Mar 6 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3437.D Vial: 49 Acq On 3 Mar 2002 11:35 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.29 ug/1 84401 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 188 C14D10 001719-06-8 91 2 Phenanthrene/d10 188 C14D10 001517-22-2 80 3 Naphthalene 6-dimethoxy- 188 C12H1202 005486-55-5 53 4 5-Oxazolecarboxamide, 2-phenyl- 188 C10H8N2O2 039819-42-6 40 Abundance 7 ‘ Scan 2267 (25.852 min): 3437.D (-) m/z 188.10 100.00% 188

5000

42 54 66 80 94 i 32 146 160 . 25.60 25*80 26.00 26.20 Tunr m/z 189.10 15.83% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d i 0- 188

5000 25.60 25.80 26.00 26.20 . 80 94 m/z 184.05 13.81% 160 00 ! I DITTTT “ 111 1’ miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180_190 Abundance - — 188 25.60 25.80 26.00 26.20 5000 m/z 8 .05 12.42% Rfi 80 94 160 00 ■ ■ i ‘ " I' “ ' i' ‘‘ i “ ■ ■ i “ “ 1111111" ' I “ “ 11' “ 1111111'1' I “ 1111'1' 11" 11 “ TTT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 1120/0/0— 188 25.60 25.80 26.00 26.20 173 m/z 94-00 10.96% 145 5000 102 114 130

mlz~> ——mmphpmt 11 " I " " I “ “ I " 76 94

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 +7 25.60 25.80 26.00 26.20

3437.D GCMS0208.M Mon Mar 25 12:25:09 2002 Page 2

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