NYC-WTC_000011460
Instrument output displaying calibration data and surrogate recovery results for sample AE03283.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration table for TCLP method, March 2002
Machine-extracted title · confidence 100%Instrument output displaying calibration data and surrogate recovery results for sample AE03380.
NYC-WTC_000011477–000011484Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\MAR0102\3380.D Vial: 44 Acq On 3 Mar 2002 6:37 am Operator : Sample gc/ms scan 2/4 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 12:06 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.32 152 782021 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 3041982 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.28 164 1586749 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.73 188 2342403 20.00 ug/1 -0.04 38) Chrysene-dl2 33.79 240 1278919 20.00 ug/1 -0.06 44) Perylene-dl2 38.07 264 835770 20.00 ug/1 -0.06
System Monitoring Compounds 37) 2,4-DDD 30.80 235 57596 2.35 ug/mL 0.30 Spiked Amount 5.000 Recovery = 47.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.72 165 187 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 3380.D GCMS0208.M Mon Mar 25 12:07:40 2002 Page 1
NYC-WTC_000011477
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