GCMS analysis results for sample AE02604, Mar 15, 2002

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Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.

NYC-WTC_000005394–000005414

Folder label: “GCMS X 2/5/02 A 3/7/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR0702\2604.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 14:24 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.31 152 479287 20.00 ug/1 -0.05 10) Naphthalene-d8 15.94 136 1874452 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.25 164 988446 20.00 ug/1 -0.07 29) Phenanthrene-diO 25.69 188 1521721 20.00 ug/1 -0.08 38) Chrysene-dl2 33.76 240 1225557 20.00 ug/1 -0.09 44) Perylene-dl2 38.03 264 915150 20.00 ug/1 -0.09

System Monitoring Compounds 37) 2,4-DDD 30.77 235 85001 5.35 ug/mL 0.27 Spiked Amount 5.000 Recovery = 107.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.99 128 822 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.65 165 236 N.D. 25) Diethylphthalate 22.72 149 459 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 2604 .D GCMS0208.M Wed Mar 13 14:24:58 2002 Page 1

NYC-WTC_000005396

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NYC-WTC_000005415

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.

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