NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 9 pages
GCMS analysis results for sample AE02761, Mar 11, 2002
Machine-extracted title · confidence 90%Laboratory report listing unknown compounds and surrogate recovery data for sample AE02761.
NYC-WTC_000005516–000005524Folder label: “GCMS X 2/6/02 A 3/1/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\MAR0102\2761.D Vial: 16 Acq On 1 Mar 2002 11:07 pm Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 10:28 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.31 152 285892 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 1110505 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.26 164 580904 20.00 ug/1 -0.05 29) Phenanthrene-diO 25.72 188 847081 20.00 ug/1 -0.05 38) Chrysene-dl2 33.79 240 595734 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 400008 20.00 ug/1 -0.07
System Monitoring Compounds 37) 2,4-DDD 30.79 235 49586 5.61 ug/mL 0.29 Spiked Amount 5.000 Recovery = 112.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.00 128 324 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 2761.D GCMS0208.M Tue Mar 05 10:29:38 2002 Page 1
NYC-WTC_000005518
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NYC-WTC_000005518Source: NYC Law Department, mirrored locally
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