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GCMS analysis results for sample AE12572, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE12572 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014700–000014709

Folder label: “GCMS X 5/28/02 A 6/4/02

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Scanned page image, NYC-WTC_000014708
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\JUN0302\12572.D Vial: 23 Acq On 4 Jun 2002 6:55 am Operator: Sample : gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 25.57 0.43 ug/1 37550 Phenanthrene-dl0 25.42 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 Anthracene-d10- / C 188 C14D10 001719-06-8(83 2 Phenanthrene-dl0y7 188 C14D10 001517-22-2 50 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 38 4 Pentacyj61o[8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 _____ 000000-00-0 38 Abundance 7 Scan 2236 (25.569 min): 12572.D (-) m/z 188.10 100.00% 118

5000

41 49 66 80 94 160 25.20 25.40 25.60 25.80 TWTPPTPTTTLNTTPPTPTTRIWIWWTLWITITTT 11- m/z 189.10 15.18% m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #19957: Anthracene-d10- 11 1118

_______ ______ 5000 25 20 25.40 25.60 25.80 ' m/z 80.00 14.10% 66 80 94 mmpm “ i " ■ ■ i “ '' i ■ “' i " “ i ■ ■ “ i ■ miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 1118 .... A........... . 25.20 25.40 25.60 25.80 5000 m/z 160.10 9.69%

80 94 160

miz-> ■ ■ i11■■ i

40 50 66 “ i1■।■ i' ■

60 70 - 80 90 100 110 120 130 140 150 160 170 180 190 l Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 108 25.20 25.40 25.60 25.80 m/z 94.00 9.65%

5000 102 115 145 130 m/z—> 51 63 75 94 119numump——*pmmhgor TTyur | rp-r 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 n. 117 ■ । ... /| .1 . T | 1 1 1 I | 1 | | | | I

25.20 25.40 25.60 25.80

12572.D GCMS0531.M Tue Jun 04 11:53:02 2002 Page 2

NYC-WTC_000014708

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NYC-WTC_000014708Source: NYC Law Department, mirrored locally

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