GCMS calibration table for TCLP method, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3282.D Vial: 42 Acq On 3 Mar 2002 4:38 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 * ... Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.28 ug/1 75798 Phenanthrene-dl0 25.72

Hit# of 5 f Tentative ID MW MolForm CAS# Qual

1 Anthracen 2 Phenanthrene-diO —69— 188 C14D10 188 C14D10 001719-06-8 83 001517-22-2 74 3 Naphthalen , 2,6-dimethoxy- 188 C12H1202 005486-55-5 47 4 Antipyrine 188 C11H12N2O 000060-80-0 38 Abundance Scan 2268 (25.861 min): 3282.D (-) m/z 188.10 100.00% 188

5000

66 80 94 132 146 158 L 25.60 25.80 26.00 26.20 —Hr | ■ i l ■ | .Ml | ■ . .I fl l . q h ll]....... ■ ■ ■ l l . 52 m/z 94.00 20.32% m/z-> 50_ 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.60 25.80 26.00 26.20 80 94 m/z 189.10 15.62% 66 160 Tpp ■ i ■ ■ • ‘ i. ‘' i ■ ■ •' i ‘ •11 ‘ “ i'1 ‘11 ■ —* T’ 3 m/z—__ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 r < •> /(bundance 188 25.60 25.80 26.00 26.20 5000 m/z .00 14.47% 80 94 160 66 ‘ " I ‘ ‘ ‘ ‘ 11 “ ' I' ‘ “ I ‘ 11'1 •11 ■1' • iu • • । ।1 ■1 • i'" • i “ •11 • • •1111 *111 ■ ■ ■ । ■ m/z--> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 25.60 25.80 26.00 26.20 173 m/z 184.10 12.38% 145 5000 102 114 130 76 94 157 | , 1' I'''' 111111''111'1'11' ।1' I ‘ “ i ‘ i ‘ • I “ ■ ■ i 1 1 1 • i “ ■' i ‘ ‘ ‘ ■ i'1'' i' ‘ 1’’ m/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3282.D GCMS0208.M Mon Mar 25 12:18:23 2002 Page 2

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