GCMS calibration table for TCLP method, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\3282.D vial: 42 Acq On 3 Mar 2002 4:38 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 1.55 ug/1 295014 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Pentanol,/ 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 4 Pentane, -methoxy- _ _ 102 C6H140 036839-67-5 9 Abundance Scan 343 (8.189 min): 3282.D (-) .. m/z... 73.00 100.0 0% 713

5000 43 11*1‘I 55 87 103 7.80 8.00 8.20 8.40 8.60 i ■ ■ ■ ■ i • ■ ■ ■ i 1 34,141 1 1 ' I ''''‘'''i > ■ ' '‘I1' Ir M ‘ 11 1 1 ' j 1 ' I **' 1 ’ l • m/ z 43.0,5 28.01%l miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 rTAIr 41111 FPPPPMi > 7.808.00 8.20 8.40 8.60 55 m/z 41.05 10.68 45 87 27 i 3.9, I I4 ' ■ ■ I , । • • • •1। • 1 • • t * ■'' ' i 1 ■ ' । • i ■ ■ ■ ■ I mz-10 20 30 40 50 60 70 80 90 100 110 Abundance 73

7.80 8.00 8.20 8.40 8.60 5000 43 m/z 44.95 10.54% 58 27 87

m/z-> 10__ 20 30 40 50___ 60 70 80 90 100 110 Abundance #292: N-Ethylformamide ' I ' ‘ ‘ ‘ I ' ‘ ' I ' ' ' ' I ‘ ‘ ‘ ' I ‘ ' 30 7.80 8.00 8.20 8.40 8.60 73 m/z 71.00 6.56% 5000 44 58

,.3. , ■ ■ 1’1 ■ 1 i 1 ■ « f » * » * 4 « * * I J * » • I I T-r-p-t m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

3282.D GCMS0208.M Mon Mar 25 12:18:18 2002 Page 1

NYC-WTC_000011517