GCMS analysis results for sample AE08688, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8688.D Vial: 10 Acq On : 22 Apr 2002 6:00 pm Operator: Sample : gc/ms scan 4/11 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.11 0.33 ug/1 42355 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 5 Abundance Scan 334 (8.109 min): 8688.D (-) m/z 73.00 100.00% 73

5000 43

87 93 103 7.80 8.00 8.20 8.40 I I 55 1........................ 1 I 1 'n ' i 1 1 1 ' 1 1 1 1 '11 । ' > ' ■ i 1 ■ ■ ■ i • ■ ■ 'iii । ' i ‘ ‘ • i ■ । । 1 m/z 42.95 34.67% m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 ■'■i■■ ■ ■ ।' । ■ ■ ■~ । ■ • ■ •। 7.80 8.00 8.20 8.40 45 55 m/z 40.95, 12.82% 27 87 I 1 39, T , , , 11 ■ । ■ ■ ■ ■ ।' 1 1.11. 1 । । । । miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 DdIa*aGaIa/a/4/08/n/a/a.m 7.80 8.00 8.20 8.40 5000 m/z 45.05, 11.12% 45

41,33.3% 55 miz-> Abundance 10 20 30 33 40 j ___ ____ ■ i • • * • i ' 50 60 #292: N-Ethylformamide T* 70

73 80 90 100 110 M. 7.80 8.00 8.20 8.40 m/z 71.00 8.24% 5000 44 58

15 - m/z—> 0 10 20 - 30, 40 50 60 । ■ ■ 1 ■ i ■ ' • 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ 70 80 90 100 110 7.80 8.00 8.20 8.40

NYC-WTC_000048950