GCMS calibration results, Feb 27 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2502\1970.D Vial: 42 Acq On : 27 Feb 2002 6:23 am Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 0.28 ug/1 23956 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 41-Butan tine, 3 - methyl - Abundance Scan 343 (8.194 min): 1970.D (-) 87 C5H13N 000107-85-7 4 m/z 73.0) 100.00% 73

5000 43 ‘ i ■ ■ 1 ■ i ‘ ■ i ■ ■ • ■ i ■ 1 ' ' I 1 '' 7.80 8.00 8.20 8.40 8.60 m/z-> ■ ■ i ■ ■ ■ ■ I 1 • ■ ■ i ■ 10 20 30 —4044 50 | 49 55 t t 1 I ■i • ' ■ ■ । ■ ■ ■ ■ । ■ 60 70 80 4r 87 90 103 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.80 8.00 8.20 ' 8.40 8.60 55 m/z 44.95 12.78% 45 87 27 3.9, | ' ' I ‘ | ‘ I ' ' ' ‘ I ' ‘ ' • l • ■ ’ ' l 114III 1. .1 . m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793. Pentanc, 3-methoxy- i 73 7.80 8.00 8.20 • ■ i ■ • ■ ■ i ■ ■ 8.40 8.60 5000 m/z 40.95 11.52% 45

27 33 39 55 1 1 T> ■ i • ■ ' , i ■ ” ‘ ‘ i’* 1

m&-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 33 7.80 8.00 8.20 8.40 8.60 73 m/z 71.00 7.14% i 5000 I 44 58 15 1 ■ i ■ ''' ' 1 1 1 । 1 1 ■ ■ la ■‘ i ■ ■ " l~i i i i j n i i । i i n । ’I j i i । i r miz-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1970.D GCMS0208.M Tue Mar 19 11:05:09 2002 Page 1

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