GCMS calibration results, Feb-Mar 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) .3 - Data File : C:\HPCHEM\1\DATA\FEB2502\1961.D Vial: 33 Acq On : 26 Feb 2002 9:28 pm Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 10:42 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. QIon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 306684 20.00 ug/1 -0.03 10) Naphthalene-d8 15.96 136 1185763 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 617627 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.71 188 861425 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 567143 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 396715 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.79 235 34805 3.87 ug/mL 0.29 Spiked Amount 5.000 Recovery = 77.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.01 128 281 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.74 149 417 N.D. 26) 4-Chioropheny1-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1961.D GCMS0208.M Tue Mar 19 10:43:37 2002 Page 1

NYC-WTC_000010403