NYC-WTC_000010409
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons on February 27, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 6 pages
GCMS calibration table for TCLP analysis, February-March 2002
Machine-extracted title · confidence 95%Calibration data file listing retention times and response factors for standard compounds used in TCLP testing procedures.
NYC-WTC_000010397–000010402Folder label: “GCMS X 1/27/02 A 2/26/02 - 3/5/02 3/20/02”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\FEB2502\1960.D Vial: 32 Acq On : 26 Feb 2002 8:29 pm Operator: Sample : gc/ms scan 1/29 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 19 10:40 2002 Quant Results File: GCMS0208.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 12.32 152 262010 20.00 ug/1 -0.03 10) Naphthalene-d8 15.96 136 1002393 20.00 ug/1 -0.04 17) Acenaphthene-dl0 21.27 164 526138 20.00 ug/1 -0.04 29) Phenanthrene-diO 25.71 188 727708 20.00 ug/1 -0.05 38) Chrysene-dl2 33.78 240 465371 20.00 ug/1 -0.06 44) Perylene-dl2 38.05 264 314812 20.00 ug/1 -0.07
System Monitoring Compounds 37) 2,4-DDD 30.79 235 34928 4.60 ug/mL 0.29 Spiked Amount 5.000 Recovery = 92.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.02 128 241 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.75 149 207 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1;2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 1960.D GCMS0208.M Tue Mar 19 10:42:02 2002 Page 1
NYC-WTC_000010397
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