GCMS sample analysis results for AE01966, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1902\1966.D Vial: 11 Acq On : 20 Mar 2002 1:45 pm Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.60 ug/1 82989 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1. 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Pent ane,/3-methoxy- 102 C6H140 036839-67-5 9 4 1 - But anamine, 3-methyl - 87 C5H13N _ 000107-85-7 7 Abundance Scan 337 (8.141 mfn): 1966.D (-) m/z 73.0.0.... 100 000% 73

5000 43 ' ' I Tt '-'V 11 ■ I ' ' • i ■ • ■ ■ i 7.80 8.00 8.20 8.40 ........................... 11.1 , 55... 11 , 11 i ' 1 ' 1 i ' 1 1 1 1 1 1 1 1 I1 11 ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ' ■ ■ 87 103 i 1 ■ ■i ' ■ ■ ‘ i ■'1 ■ ■ i ■ m/z 42.95 30.88% m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 * * । * * * < i * * 7.80 8.00 8.20 8.40 55 m/z 44.95 11.57% 45 87 27 39, | | m/z-> 1 ■ j ■ ■ ■ 10 ■ i • • ■ ■ I' ■ ■ ■ i‘ ■ 1 ■ i ‘ 20 30 40 50 i ■ 1 ■ ■ i ■ 60 70 1. 80 .1 90. 100 110 Abundance 30 73 A 7,80 8,00 8.20 8.40 5000 m/z 4!.05 9.66% 44 58

15 1II0* m/z-> 10 ..20___ 30___40___ 50__ 60 .. 70 80 90___ 100__ 110 Abundance #1793: Pentane, 3-methoxy- A--A4 ........ 73 7.80 8.00 8.20 8.40 m/ z 71.00 6.90% 5000 45

............ 27 33 39, 55 —PP—t 1 ■ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ■ ■ • ■ i ‘ . .. A m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 ''1

1966.D GCMS0308.M Thu Mar 21 09:17:19 2002 Page 1

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