GCMS compound summary for sample AE01437, Feb 2002

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Summary of gas chromatography-mass spectrometry analysis results for sample AE01437 processed on February 21, 2002.

NYC-WTC_000009869–000009876

Folder label: “GCMS X 1/22/02 A 2/22/02”

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Data File : C: \HPCHEM\1\DATA\FEB2102\1437.D Vial: 9 Acq On : 21 Feb 2002 9:59 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.36 ug/1 25592 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 4 3 Pentane ,/ 3 -methoxy- 102 C6H140 036839-67-5 4 4 1,3-Dioxolane, 2-methyl- 88 C4H802 73.00 100.00% 4 000497-26-7 Abundance / Scan 345 (8.206 min): 1437.D (-) m/ z 73

5000 43 _________; ____ _ _____ I ‘ ‘ ‘ ‘ I ' ‘ ‘ ‘ I ' ' ' ‘ I ‘ ‘ ‘ I ‘ '

391 | 51 55 69. , 84 87 7.80 8.00 8.20 8.40 8.60 ■ • i ‘ “ i" ■ • i ■ “ ■ i •" ■ i" - TITTTIWTNTTTITTTT m/ z 42.95 34.89% m/z~> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63573: 3-Pentanol, 3-methyl- 7)3

5000 55 7.80 m/ z 8.00 44.9,5 IW 8.20 8.40 12.66% 8.60 , 27 31 41 45 87 84■ i ‘1| " i "'' i'' 69 TImTTTHTTTIn’tt >111< < >1J ri> t J >11 i |1> • ' i ‘ miz— 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/ z 40.9 10.26% 44 58 27 15 41 ■ “ ■ ।" i ■" ■ i" ■ ■ i ■ “ ■ i ■ ■ ■11 ■ ■ • ■ i" ■ • i ■" ■ ।" ।11 ■11 ■ • i ■ ■ ■ ■ i" " ।■ i'' i" ■ ■ i ■ ■ ■ ■ i ■ 1 mfe->___ 5 10L 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 .... .................. Abundance #1793: Pentane, 3-methoxy- 73 7.80 8.00 8.20 8.40 8.60 m/z 71.0.0 7.77% 5000 41 45

27 . 55 59 70 11 ■ ■" i ■" ■ i ■ ■ ■ ■ ।1 “ ■ i Irr TIuutpmnonttt i ‘ • i ■ ‘ ‘ ' I 1 ' ‘ ' I ‘ 1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1437.D GCMS0208.M Fri Feb 22 09:32:10 2002 Page 1

NYC-WTC_000009872

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