GCMS calibration table for sample AE09448, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0202\9448.D Vial: 7 Acq On 2 May 2002 8:39 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.09 0.68 ug/1 53049 1,4-Dichlorobenzene-d4 12.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 25 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Penta: 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance Scan 333 (8.089 min): 9448.D (-) m/z 73.10 100.00% 73

5000- 43 I । । > । । । t i । ii । r [ ‘rv । i । i ।

7.80 8.00 8.20 8.40 .............................. . T । । i । i । i i i i । I i I I | I I i r | i i । ' i 1 ._______I I ' । I i i । i I 87 i । । । । । । | 103 1l i T i m ।—| 1 m/z 43.05 32.01% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000- 7.80 8.00 8.20 8.40 55 m/z 41.10 12.16% 45 87 ....... 27,39 150 ' I 1 ' 1 ' I 1 ' 1 '“I 1 ' ' 1 1 1 1 1 ‘ 1 1 - m/z-> 10 20 30 40 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73

7.80 8.00 8.20 8.40 5000- m/z 45.05, 10.86% 45

........................ 36 il 55 TPHu ' i 1 ■ 67 ................... 109,115, m/z-> Abundance ■ ' i ■ ' ' ' i ' ' 1 1 i 1 ' 1 ' i 1 10 20 30

30 40 50 60 ' 1 i 1 70 80 #292: N-Ethylformamide 90 100 110 120 hA 7.80 8.00 8.20 8.40 73 m/z 71.10 6.71% 5000- 44 58

15 1 i 1 ' 1 1 i 1 —P—TT । । । । । । । । it ii । i i i i [“I r

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

9448.D GCMS0501.M Fri May 03 08:41:05 2002 Page 1

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