GCMS analysis results for sample AE04039, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4039.D Vial: 20 Acq On : 23 Mar 2002 2:47 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.15 3.90 ug/1 439805 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Silane/ tetramethyl-______ ___ _____ 88 C4H12Si 000075-76-3 9 Abundance Scan 338 (8.147 min): 4039.D (-) m/ z 73.0,0 100.00% 73

5000 43 । । । 1* । . , . । । । 7.80 8.00 8.20 8.40 37, |, . .......................... . > 87 1 103 * ‘ I , r’ 1*I4* 114 i • ■ i ‘ m/z 43. 5 27.33% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 **/1*1* *n 1**1* 7.80 8.00 8.20 8.40 55 m/z 45.05 10.70% 45 87 27 I 39 : ' *■»!><» <‘| < 1 1 ‘ t ' m/z-> Abundance • * i ‘ 1 ‘ ‘ i ' ‘ ‘ ‘ i ‘ ‘ ' 1 T' ■ ■ > | 10 20 30 40 50 60 70 #292: N-Ethyifrmamce 80 ' I 1 ‘ ‘ 1 I ‘ ‘ ‘ ■ I ■ ‘ ‘ ‘ I ‘ ‘ 90 100 110 120 30 73 -I-P 7.80 8.00 8.20 8.40 5000 m/z 41.05 10.46% 44 58 15 . 1 mhmP m/z-> 10 20 30 40 __ 50 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet ■ ■ rfi ' ‘ Potru । Pi ■ ■ । ■ 73 7.80 8.00 8.20 8.40 m/z 71.00 7.08% 5000 45 36 55 • i ■ ■ ■ ‘'i 1 + 14**** I 1a J TTPTrrmT i i • I 1 ' ‘ i ■ 67, 109115 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

4039.D GCMS0308.M Wed Mar 27 10:00:51 2002 Page 1

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