GCMS analysis results for sample AE04039, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4039.D Vial: 20 Acq On : 23 Mar 2002 2:47 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

21.10 0.22 ug/1 36690 Acenaphthene-dl0 21.21

Hit# of 5 Tercative ID MW MolForm CAS# Qual

I Cyclopentanone 84 C5H8O 000120-92-3 27 2 Furan, 2,5-dihydro-3-methyl- 84 C5H80 001708-31-2 27 3 1,9-Diami nononane 158 C9H22N2 000646-24-2 16 4 2H-Pyran, /3,4-dihydro­ 84 C5H80 000110-87-2 16 Abundance ........ .. ..... Scan 1749 (21.100 min): 4039.D (-) m/z 55.00 100.00% 55

5000 84 129 41 111 —mAttt ++ndmnptomtp 71 101 20.80 21.00 21.20 21.40 - ’ I,... ’ ’ 1 ‘1 141 156 172 m/z 84.00 40.17% miz-> 20 30 40..50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #558: Cyclopentanone 55

5000 84 i I | j i l l 184 I f | 11 1 19 1 11 20.80 21.00 21.20 21.40 27 m/z 129.00 32.01% 42 67 /____________ _________________ ■। ‘ । ■ 1,1 i ■ 1 " i 1 ■ i “ ' ‘ i • " ■ i ■ f' ■ i' “ ‘ i ■ " ‘ i ■ ■ ■ ■ i''1 ■ i “ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■' “ i ■■ ■ ■ i1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance -/5 Furata 2.5- byor-3-methyl 29 41 t

84 A 20.80 21.00 21.20 21.40 co 69 5000 56 m/z 111.00 26.69%

;, 49 •112m0111011001110011/017—s -mIm002102199211100mm"[ mlz~> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #12012:1,9-Diaminononane T T T 30 20.80 21.00 21.20 21.40 m/z 41.05 26.27% 5000

4 56 gg 86 100 114 129 142 12*WTP]mma——un—hmmmOmmm*TmPPTTIT 11 ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 20.80 21.00 21.20 21.40

4039.D GCMS0308.M Wed Mar 27 10:00:55 2002 Page 2

NYC-WTC_000011736