GCMS analysis results for sample AE04024, Mar 15 2002

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Data File : C:\HPCHEM\l\DATA\FEB2102\4024.D Vial 79 Acq On : 24 Feb 2002 11:45 pm Operator Sample : gc/ms scan 2/22 Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************** * * * * * * * * * **************** Peak Number 3 1,6-Dioxacyclododecane-7,12-di Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. .

21.17 0.27 ug/1 25782 Acenaphthene-dip 21.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1, 6-Dioxacyclododecane-7 ,12-dione200 C1OH1604 000777-95-7 40. 2 Cyclopentanone 84 C5H80 000120-92-3 32 3 2H-Pyran, 3, 4 - dihydro - 84 C5H80 000110-87-2 27 4 Hydracryli acid, monoanhydride wit 156 C7H13BO3 033823-94-8 23 Abundance Scan 1757 (21.173 min): 4024.D(-) m/z 55.00 100.00% i 55

5000 84

41 100 m 129 TT A IT

miz-s • I''" I' JU - 71 156 TTrHT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 m/ z 21.00 21.20 21.40 21.60 84.05 48.79% ■ Abundance #22852: 1,6-Dioxacyclododecane-7,12-dione 55

5000- 27 84 I ' 1 ' 1 1 1 42 20.80 21.00 21.20 21.40 21.60 100 71 129 m/z 111.00 26.69% ’ I " '' I •" ' i _.. I T‘0‘ 111" ‘ I" " I' ‘ i 111 200 I r172 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 'Abundance #558: Cyclopentanone i 55 ‘d yr 20.80 21.00 21.20 21.40 21.60 5000 84 m/z 129.00 25.10% 27 42 _ ......... :................ 67 T‘‘E‘IEEEI[‘E"TT 11 < । < 11 > < > > 111 > < 11 TTTTT’IIT I' •" i i" " i1 ”' i ■' ’ ■ i 1" ‘11 m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #62717: 2H-Pyran, 3,4-dihydro- TI TT 55 20.80 21.00 21.20 21.40 21.60

84 m/z 56.00 25.06% 5000 27

69 I ! ITTTTTTTTTT tW I' •" I ‘I, i ■'" i ■ ■ ■ ■ i" " r1 ■ H " i ■ •" i" ■ ■ i • ■' ■ r ’r"■i TI 1IT IT miz-> 20 30 40 50 60 70 80. 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40 21.60

4024.D . GCMS0208.M Wed Mar 13 11:39:09 2002 Page 3

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