GCMS analysis results, Sample AE05750, April 18, 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1202\5750.D Vial: 19 Acq On : 16 Apr 2002 1:43 am Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2H-Pyran, 3,4-dihydro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 21.06 0.23 ug/1 46333 Acenaphthene-dl0 21.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Pyran, 3,4-dihydro- 84 C5H80 000110-87-2 22 2 Ethyl 9-decanoate 198 C12H2202 000000-00-0 14 3 Cyclopentanone 84 C5H80 000120-92-3 12 4 Cyclodecanone 154 C1OH180 001502-06-3 12 Abundance Scan 1744 (21.059 min): 5750. D (-) m/z 55.00 100.00% 55

5000 84

41 100 111 129 A m/z—> ll 44 ‘1 r............... 7.. 156 141 ■ ■111"1' ।'" ■ ।1'111" ■' ।11 ’' ।1" ■ ।'" ■ ।" ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40 m/z 83.95 A 46.67% Abundance #62715: 2H-Pyran, 3,4-dihydro-

84 /MA AMA,A /111M4 4m A/ 5000 27 20.80 21.00 21.20 21.40 m/z 129.00 30.24% hi 69 .. 1111...... I......... m/z-> 20 on '11111 11111'11111111 " " "i"" ■■ "i11"1 'i"" i" " 11111" " " "i" " i i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 i i i

Abundance #22384: Ethyl 9-decanoate 55 88 69 20 80 21.00 21.20 21.40 5000 101110 m/z 111.00 27.14%

123 135 152 ' r111111" i'1" i ■" ■ ‘ I‘ ll 11 I’T IITT 1110010—0001101300117 TICIUIBBTT 198 m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #62725: Cyclopentanone L 20.80 21.00 21.20 21.40 m/z 41.05 23.97% 84 5000

41

....... '.Lr r "' i " " I i " " i " " r 1" r " 11" " i " " ir " 1 r 1" r " 11" 11 r "11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 20.80 21.00 21.20 21.40

5750.D GCMS0412.M Wed Apr 17 09:46:58 2002 Page 3

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