GCMS analysis results, sample AE04734, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR28O2\4734.D vial: 7 Acq On : 28 Mar 2002 2:28 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

21.08 0.26 ug/1 41116 Acenaphthene-dl0 21.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanone 84 C5H8O 000120-92-3 35 2 Hydracrylic ^cid, monoanhydride wit 156 C7H13BO3 033823-94-8 25 3 2H-Pyran, 3y4-dihydro- 84 C5H8O 000110-87-2 25 2'3, 4,5-Te^ahydrop_yridazine 84 C4H8N2 000694-06-4 22 ■Abundance 7 ’ Scarf1746121)0781^^ m/z 55.00 i 5 i

84 5000 41 100 111 129 ....... ly.-....... m/z-> 20 30 40 50 60 71

70 4^ 80 7 90 100 110 I i‘l I....... ... 141 120 130 140 150 160 156 m/ z 20.80 21.00 21.20 21.40 84.05 53.40% 'Abundance #62725: Cyclopentanone 56

84 ^z\Aw7^v-Af-\AA/\/^ 5000 V r 20.80 21.00 21.20 21.40 41 m/z 111.0,0 27.61%

m/z->____ 20 30 I 40 50 60__ 70___ 80__ 90 100 110 120 130 140 150 160 Abundance #11340: Hydracrylic acid, nionoanhydride with i-butanebororii i 55

20.80 21.00 21.20 21.40 5000 m/z 56.00 27.53% 99 72 “ 128 H 114 I' 156 __ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ■Abundance #62716: 2H-Pyran, 3,4-dihydro- j\ I 5 20;80 21.00 21.20 21.40 27 m/z 129.0.0 26.88% 5000 84 39

69 ■ ......... I I I , 'm/z-> 20^ ' I ' ' ‘ ' I ' ' ' ' I ' ■

30 40 50 60 70 80 90 100 110 120 130 140 150 160 2a80 21.00 21.20 21.40

4734.D GCMS0308.M Mon Apr 01 10:06:24 2002 Page 1

NYC-WTC_000058281