GCMS quantitation results for sample AE10242, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020516\10242.D Vial: 18 Acq On : 17 May 2002 2:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Cyclopentanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 24.61 0.51 ug/1 34479 Acenaphthene-dl0 24.45 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanone 84 C5H80 000120-92-3 43 2 2H-Pyran/ 3,4-dihydro- 84 C5H80 000110-87-2 43 3 2-Ethylacrolein 84 C5H80 000922-63-4 43 4 1,6-Dioxacyclododecane-7, 12-dione 200 C1OH1604 000777-95-7 40 Noundance Scan 3665 (24.613 min): 10242.D (-3657) (-) m/z 55.05 100.00% 55

5000

n 84 41 111 T-I4

n/z-> Abundance 10 20 30 40 50 71 1 —H + -H 129 100 | 156 ’I—001011—00—V0nan 60 70 80 90 100 110 120 130 140 150 160 #111215: Cyclopentanone I. 24.20 24.40 24.60 24.80 25.00 m/Z 84.05 39.13%

55

5000 28 41 84 "MMWY W Mhyrh 24.20 24.40 24.60 24.80 25.00 m/z 41.10 31.57%

/z-> ........ r‘ ' | 1 10 20 I“ 1 30 4., 69 ' i11 ■1111' ‘ i ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #14359:2H-Pyran, 3,4-dihydro-

24.20 24.40 24.60 24.80 25.00 27 84 m/z 111.10 23.22% 5000 39

Tr -l—4l 4 69 15 ■ ■ ' । ■ ' । ■ ■ '' i " " i " " i " i " ... ............... ... । [ 11111 ■ । n/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 55 #14365:2-Ethylacrolein I 1 24.20 24.40 24.60 24.80 25.00 84 m/ z 56.00 22.68% 5000 , 29 39

/z—> -19-1l—4u4u 10 20 30 40 50 69 "TTT 60 70 80 90 100 110 120 130 140 150 160 TIT ' ■ i ' ■ 24.20 24.40 24.60 24.80 25.00

10242.D SCAN020507.M Fri May 17 10:41:21 2002 Page 5

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