GCMS quantitation results for sample AE10242, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\10242.D Vial: 18 Acq On : 17 May 2002 2:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 4 R.T. EstConc Area Relative to. ISTD R.T. 15.46 0.34 ug/1 22619 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 25 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 23 3 N-(Irifluoroacetyl)-O,O',O''-tri... 481 C19H34F3NO4Si3 1000072-26-3 17 4 3-(2-Methoxyphenoxy)lactic acid,... 356 C16H2805Si2 1000072-00-0 9 Abundance Scan 2107 (15.459 min): 10242.D (-2095) (-) m/z 73.00 100.00% 73

5000 267 355 A 43 , Il l I , I I r 1 1 1 1 50 r 1 i > ' 1 1 । 1 t 1 i 1 1| 100 150 200 250 300 350 i...... .400 450 15.20 15.40 15.60 15.80 m/ z 267.00 26.75% Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 < ■ i ■ ■ > ■ i ■ ■ ■ ■ i ■ ■ 15.20 15.40 15.60 15.80 355 m/z 354.90 23.77% 45 . . I , , 96 ' 'i 1 ' 133 165, 193 4‘1 'i 114 77,223244 +,293 ,323, L n/z-> 50 100 150 200 250 300 350 400 450 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 15,20 15.40 15.60 15.80 267 5000 m/z 356.10 19.25%

45 11— 207 011.11323,, L n/z-> Abundance 50

73 100 150 200 250 300 350 400 #27960: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)n... 450 । i-| ' । । । I ’ 1... 15.20 15.40 15.60 15.80 m/z 74.00 16.51% 355 5000

45 |, 126147170193 ' 'i 1 1 ————————————————————— 236 265286 1376 481 n/z-> 50 100 150 200 250 300 350 400 450 15.20 15.40 15.60 15.80

10242.D SCAN020507.M Fri May 17 10:41:20 2002 Page 4

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