NYC-WTC_000025542
Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis results for sample AE10812, May 2002
Machine-extracted title · confidence 100%Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
NYC-WTC_000025520–000025532Folder label: “GCMS X 5/17/02 A 5/16/02”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\10812.D Vial: 18 Acq On : 22 May 2002 1:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamet... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 15.45 0.28 ug/1 26260 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual —1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 32 3 N-(Trifluoroacetyl)-N,0,0',O'‘-t... 553 C22H42F3NO4Si4 1000072-26-7 12 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 9 Abundance Scan 2105 (15.447 min): 10812.D (-2095) (-) m/z 73.10 100.00% 73
5000
267 355 116 157 191 223 15,20 15.40 15.60 15.80 0- i 49 .Hi I , I 1,1, , ,i i, 1 , Ji 1, ,1, , J ,»......... .. m/z 355.10 25.56% 11T ■ 1 nz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115315: Cyclopentasiloxane, decamethyl- 73
355 267 i.............. A 5000 ■ ■ i - ■ • 1 i ■ ■ ■ ■ i 1 ' 15.20 15.40 15.60 15.80 m/z 267.00 21.90% 45 207 323 i । 0- ■ ■ । < /* TPT TI । miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115273: Cyclopentasiloxane, decamethyl- 73
15.20 15.40 15.60 15.80 5000 267 m/z 59.10 14.32% 355 45 Ol i , 1 1 r 103 133 165 193.223 . 293 323 , 1111 ' ' i ■ ■ ■ ■ i ■ 1 ' ■ i ■ ' ' ' i ■ ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27961: N-(Trifluoroacetyl)-N,O,O',O”-tetrakis(trimethyls... • ■ i ■ - 1 1 I 1 1 1 ‘i 1 1 73 15.20 15.40 15.60 15.80 m/z 355.90 14.15% 355 5000
45 —1 116 147 193 236 267 h............... 538 O-r rfr l 1 1 ■ ■ i ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 15.20 15.40 15.60 15.80
10812.D SCAN020521.M Fri May 24 09:21:54 2002 Page 6
NYC-WTC_000025529
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NYC-WTC_000025529Source: NYC Law Department, mirrored locally
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