GCMS quantitation results for sample AE10247, May 2002

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Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.

NYC-WTC_000024896–000024906

Folder label: “GCMS X 5/14/02 A 5/17/02”

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Data File : C:\MSDCHEM\1\DATA\020516\10247.D Vial: 23 Acq On : 17 May 2002 7:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.47 0.31 ug/1 23125 Naphthalene-d8 16.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 43 4 Benzeneethanamine, N- [ (pentafluo. . . 475 C21H26F5NO2Si2 055429-85-1 32 Abundance Scan 2108 (15.465 min): 10247.D (-2096) (-) m/z 73.10 100.00% 73

5000 267 355 ■ * i ■ ■ i ■ 1 ■ 1 1 1 1 15.20 15.40 15.60 15.80 47 103 193i1 ■ ■ • i" " i 251 1 'i i " 111" 11 ’1 ‘ i" " i1 ‘" i" " i' ' i"1' i " " r ‘r TT rr^+r m/z 266.90 37.29% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 15.20 15.40 15.60 15.80 m/z 355.10 32.89% 45 191207223 251 i 323339 TTBa01u*uanmmmCmmOM—Tm0102000100000t 11J J' ■ i" 'i" T’’ /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

15.20 15.40 15.60 15.80 5000 267 m/ z 356.20 15.84% 355 45 .2.1S 96.115 133149165, 193, 223.2 4 307323339.1,., ■ ■ " I'1' ’ i " " r •' • i "'11" ' ■ i ■ ■ " i ■ " ' i ■ /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #27659:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 15.20 15.40 15.60 15.80 m/z 267.90 14.06% 267 5000 179 356 45 147 28 1 m/z—> T —103131 1163. ITTTi 20 40 209 ;237 , 1111 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 । 312 ■ > i ■ ■ • > । 15.20 15.40 15.60 15.80

10247.D SCAN0205O7.M Fri May 17 10:49:54 2002 Page 4

NYC-WTC_000024903

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