GCMS quantitation results for sample AE10247, May 2002

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Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.

NYC-WTC_000024896–000024906

Folder label: “GCMS X 5/14/02 A 5/17/02”

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Data File : C:\MSDCHEM\1\DATA\020516\10247.D Vial: 23 Acq On : 17 May 2002 7:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ******************************************************* * * ************ Peak Number 3 2-Propen-1-one, 1-(2-hydrox... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.09 0.27 ug/1 22094 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propen-l-one, 1-(2-hydroxy-3-m... 192 C11H1203 040992-03-8 59 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 53 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 53 4 2,4-yDiamino-6- (hydroxymethyl) pte. . . 192 C7H8N6O 000945-24-4 45 Abundance | Scan 4768 (31.094 min): 10247.D (-4759) (-) m/z 192.10 100.00% 192

5000: 8

30.80 31.00 31.20 31.40 49 86 96 106 118 " r'" i" " i" " i" " i'1" i" " i" " i" " i1 ‘11 r11' i1"' i ‘‘11" " I" " I"1' 1 ■"11'" ‘ i" " i" " I 146 1 60 | HTm m/z 191.10 16.35% mz-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80998:2-Propen-1-one, 1-(2-hydroxy-3-methoxy-6-methylphe... 192

165 177 5000 131 30.80 31.00 31.20 31.40 55 65 77 103 m/z 146.00 13.58%

............. 7l. 91. 4 121 149 ' 1 | ' 1 1 » | i i ' | i ' । i J > n : | • i । ' |T i n । r il i । i i > i । ) i ■ » | 1 I r : | i i i 1 1 I •" ।" i ■111" ■

m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192

30.80 31.00 31.20 31.40 5000 m/ z 95.90 11.94%

। । | । । ' 11 I I, | | | 45 “f,90 108 122 134 148 160 | 111" | 1! 111 I1! I J| 11 I! | I| 1. | ... 11 11 I > | I >> I | I III 111 rHTT I 11 I'l I ( I < H | I < ( < | ’ ’1’4 m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate ' 1 i ■ ' ■ ' i ■ ■ TET 19/2 30.80 31.00 31.20 31.40 m/z 193.10 9.74% 64 5000

39 50 75 90 134

m/z— > -4..18.24H4+H + 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 ++tr 1 107 hmmp 122. , 148 160 30.80 31.00 31.20 31.40

10247.D SCAN020507.M Fri May 17 10:49:54 2002 Page 5

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