GCMS sample analysis report AE08483, May 7 2002

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Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

NYC-WTC_000048623–000048634

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08482.D Vial: 19 Acq On : 20 Apr 2002 1:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Thiocyanic acid, 2-benzothi... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.34 ug/1 736271 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Thiocyanic acid, 2-benzothiazoly ... 192 C8H4N2S2 006011-99-0 45 2 2-Propenal, 3-(3,4-dimethoxyphen. . . 192 C11H1203 004497-40-9 40 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 40 4 6,2,5-Ethanylylidene-2H-cyclobut... 192 C11H120S 019086-86-3 37 Abundance Scan 4767 (31.088 min): 08482.D (-4756) (-) m/z 192.10 100.00%| 1912

5000 40 30.80 31.00 31 JO 3L40' miz-> 20 ■ i“ Mi ■ 54.. 7082%6......... 146 160..... | ll++p . i.. (. ।, 1, I,,,. 111,. ।. II. 11111 [Tl 11 [ 11111111111111111111 itrt 11111 30 40 50 60 70 80 90 100110 120 130 140 150 160170 180 190 200 ■ । J1 m/z 40.10 25.41% Abundance। #80870: Thiocyanic acid, 2-benzothlazolyl ester 192

5000 30.80 31.00 31.20 31,40' 69 ino 134 m/z 191.10 18.22

n/z—> 20 -m##K.Ml—HRRMRM?L4199 E 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 . Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyi)- 1:2 161 30.80 31.00 31.20 31.40 5000 m/z 146.10 14.66 77 91 . 121 149 177 d+ 1.799.. .. ,... ...... . 52 64

miz-> 20 30 40 50 60 70 80 90 100110 120130 140 150 160170 180 190 200 Abundance #125848: Anthracene, 9-methyl- • ■ i ■ ■ ■ ■ i ■ i ■ ■ ■■ i ■ ■ 1:2 30.80 31.00 31.20 31.40 m/z 96.10 12.89 A 5000-

96 A 27 39 51 63 74 82 l 115 126 139 152 ,| 176 „ | | 11 r ■ • *11 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 2(X) ■ ■ । ■ ■ ■ ■ ।■ 30.80 31.00 31.20 31.40

08482.D SCAN020418.M Thu May 02 11:44:33 2002 Page 6

NYC-WTC_000048632

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NYC-WTC_000048632Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE08488, May 2002 · Box DEP Box 27

NYC-WTC_000048660

Laboratory report documenting GCMS analysis of sample AE08488 conducted on May 7, 2002, by analyst DLV.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998