GCMS analysis results for sample AE08488, May 2002

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Laboratory report documenting GCMS analysis of sample AE08488 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048660–000048671

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08486.D Vial: 23 Acq On : 20 Apr 2002 5:47 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Phenanthrene, 2-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.28 ug/1 593196 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 53 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 45 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 4 2-Imidazolidinone, 1-methoxy~3-p... 192 C10H12N2O2 052420-43-6 40 Abundance Scan 4767 (31.088 min): 08488.D (-4756) (-) m/z 192.10 100.00%| 112

5000

40 52 64 82 * 122 146 160 I 30.80 31.00 31.20 31.40 > 11 > 1111 > 11 pl i > 11111 । > I /111 j 11 j 1111111111! t 1111111111111111111 irr 11 j !’| r I tT| i J11 j 1111 Tr j 111 r m/z 191.00 15.09 n/z-> 20 30 40 50 60 70 80 90 100110120130140150 160 170180 190 200 Abundance #125842: Phenanthrene, 2-methyl- 19/2

5000 30.80 31 ‘do 31*20 31.40 ' m/z 96.10 14.23%| 96 27 39 51 63 82 J 115 126 139 152 165 176 Thmm—ummmommnhgmmmmRTpanum—apgmmgr 1 | 165 176 niz-> :2030405060 70 8090 100 110 120130140 150160 170 180 190 200 Abundance #125848: Anthracene, 9-methyl- 112 A 1 '"I >ii'i ‘314—r‘IUI 30.80 31.00 31.20 31.40 5000 m/z 146.10 13.02

96 . 27 39 51 63 82 1 115 126 139 152 100 176 J ( 11 ‘ 1111. ■1 T 1 n 11ATr । I'll I'ft "f r 1111111 rr 11111111 n i'| 1,: > |'I ■ ■ ■ plr’t i (1 rh 111 i'|l|llli ।, [, । rnfz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 1«) 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 112 30.80 3100 31.20 31.40 m/z 193.10 12.37 5000

„ 69 90 108 134 . 45 I I i , I , | 122 | 148 160 . H ..., (■ l‘i 1 11 ■ 11 I A I 1, 11 [ 111 ■ 11 ■ 11! ■ In 11111 |T| 11 (11,,, Ipme n'l I ni u 11 n 11 I'm 111 ( 1 1T'1 1 ' 1 1 1 1 1 | ' 1T 1 I 1 I m/z—> 2030405060 70 8090 100110 120 130 140150160 170180 190 200 30.80 31.00 31.20 31.40

08486.D SCAN020418.M Thu May 02 11:56:40 2002 Page 6

NYC-WTC_000048669

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GCMS sample analysis report AE08483, May 7 2002 · Box DEP Box 27

NYC-WTC_000048623

Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

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