GCMS analysis results for sample AE08488, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08486.D Vial: 23 Acq On : 20 Apr 2002 5:47 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene -dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 762847 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

±—Anthi adene - dx 0 - 188 C14D10 001719-06-8 64 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Benzaldehyde, 2,5-difluoro-4-hyd... 188 C8H6F2O3 148872-77-9 37 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 33 Abundance Scan 4915 (31.957 min): 08486.D (-4904) (-) m/z 188.15 100.00% 188

5000 40 94 80 ‘I ■ i > । , , — । > > । pi । । i [ । 31,60 31.80 32.00 32.20 49 66 , 136146 160 ■i "■ ‘i “' ■ i‘1 “ PmmHpt •I 111.11111111111111 > | 7| 1 r > I n 111H I > 1111! 11 i ■■ ■■ i m/z 40.10 24.56 miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79826: Anthracene-d10- 108

5000 t i 1 • ■ ■ i ' 31.60 31.80 32.00 32.20 rn/z 94.05 19.85 80 94 160 । 17 30 42 52 IOnmmTHnmpmmm P . J 108118 132 146 . |,| 1701791 miz-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188 ‘ | ■ r I । O । ■ i i i । i । i j । r 3160 31.80 32.00 32.20 5000 m/z 189.20 17.26%

80 94 160 42 52 66 11 108 118 132 146 .. 170179,,I 1111. । m 11 ■ i. 1111111H111111111111 11111— miz—> 10 20 30 40 50 60 70 80 90 100 110 W130 140 150 160170 180 190 ' Abundance #79822: Benzaldehyde, 2,5-difluoro-4-hydroxy-3-methoxy- ’T ■ ‘ ' i ■' 11 i ■ ■ ■ • । 11 ' 1 i1 18 8 31.60 31.80 32.00 32.20 m/z 80.10 13.77 5000

43 57 69 79,88 97,108117 128 J 159 172 [ D xisjokaegonui g ifl’e A »rT’rreeg’rt’egrv’’’ ! । rrel’ 11 retpea m riri । rrr’p j r ’ । j 11 r’l n j 11' TT ----- iz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 31.60 3180 32.00 32.20

08486.D SCAN020418.M Thu May 02 11:56:41 2002 Page 7

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