GCMS chromatographic data for sample AE10302, May 28, 2002

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Data File : C:\MSDCHEM\1\DATA\020516\10302 .D Vial: 25 Acq On : 17 May 2002 9:03 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Anthracene-diO- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.31 ug/1 25013 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 80 2 Phenanthrene-diO 188 C14D10 001517-22-2 72 3 Benzaldehyde, 2,6-difluoro-4-hyd... 188 C8H6F2O3 1000116-28-9 9 4 80\.mino-6-methoxy-3-methylquinoline 188 C11H12N20 1000214-47-4 9 Abundal Scan 4915 (31.958 min): 10302.D (-4905) (-) m/z 188.20 100.00% 188

5000

* i ’ 1 ' • I • 1 '1 i 1 1 1 1 i ' 1-1-1 i 1 31.60 31.80 32.00 32.20 49 64 80 94 104 160 TI—I—UUTTTTT11uumuutumm | m/z 189.20 23.17% i" " i mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 108

5000 JI......... 31.60 31.80 32.00 32.20 m/z 184.20 13.44% RR 80 94 1 60 ,

n/z-> +1739,42..52..fF,.4+.#+l.7108.118.132.146 —179179/. 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 1,

Abundance #79827: Phenanthrene-d10 188

ITIBB/nIuruI.m 31.60 31.80 32.00 32,20 5000 m/ Z 94.10 11.07%

94 80 160 30 42 52 66. || . 108 118 132 146 I 170179.1,1 ■i " "i " 111" 111"‘ '111" 1111' ITTF '1 I"I Ijl I I I I ! I I I | I I I I I I I I I I I I I I | I I 1 I | I iTl'p I I I | I I I I | l'lllll'| I I I II n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 Abundance: #79823: Benzaldehyde, 2,6-difluoro-4-hydroxy-3-methoxy- 118 31.60 31.80 32.00 32.20 m/z 160.10 9.34% 5000 173

/z—> 478.7.2.%7zos722—"45ss—., 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 p 31.60 31.80 32.00 32.20

10302.D SCAN020507.M Fri May 17 10:54:13 2002 Page 6

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