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GCMS analysis results for sample AE11281, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11281 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024706–000024718

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11281.D Vial: 15 Acq On : 16 May 2002 1:38 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.95 0.39 ug/1 42393 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 86 2 Phenanthrene-diO 188 C14D10 001517-22-2 47 3 ^Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 40 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 40 Abundance Scan 4914 (31.952 min): 11281. D (-4904) (-) m/z 188.20 100.00% 188

5000

44,54 66 80 44 158 ------- .... 146 1171 L »• i111«।«i *»। > i«111 * t»i >«। q»।1 • i • • ‘ 11 *1 r 31.60 31.80 32.00 32.20 m/z 189.10 17.80% miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

5000 31,60 31.80 32.00 32.20 m/z 184.10 17.35% 80 94 160 , . 66

miz-> 1| 17 | । 30 42 52 108118 132 , I I 1 ■ ' I | I । ! 11111111111 11111 T1—B——mmpughmtm 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ‘I 146—+179179. Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/z 187.10 16.06%

80 94 160 30 42 52 66 111 " 11111 r J " E11 >'111111111111111 H 1111 +108.118.132.146—4.1791791—— TI mlz-> 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 190 Abundance #79744:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 31.60 31.80 32.00 32.20 m/z 158.10 13.38%

5000 121

173 -an 39 50 67| , 82 94I, 108 | 134 146 161 | - ■ i"' ‘ i" " i" ■ 'i1" Iri" i11111rl ■' ।' i111"1111 1 " l'1'"' I' " ■!' .I1'! "“r'l''l " I' ■ 11....... “ 'l m/z—> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 31,60 31.80 32.00 32.20_____

11281.D SCAN020507.M Thu May 16 10:01:01 2002 Page 7

NYC-WTC_000024716

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NYC-WTC_000024716Source: NYC Law Department, mirrored locally

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