GCMS analysis results for sample AE11281, May 2002

NYC 9/11 Public Portal Document Llbrary aearen compound Report

Data File : C:\MSDCHEM\1\DATA\020515\11281.D Vial: 15 Acq On : 16 May 2002 1:38 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Decanedioic acid, bis(2-eth... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 42.54 15.33 ug/1 976879 Perylene-d12 43.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual — 1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 45 2 dl-2-yEthylhexyl chloroformate 192 C9H17C1O2 024468-13-1 43 3 3 -Piperidinone, 1-acetyl-6-methyl- 155 C8H13NO2 054751-97-2 27 4 Cyclopentane, 1,2,3-trimethyl- 112 C8H16 002815-57-8 22 Abundance Scan 6716 (42.540 min): 11281 .D (-6702) (-) m/z 185.20 100.00% 517 185 —_

5000 112 83

143 42.20 42.40 42.60 42.80 -T-Y —P 14,44 J ..... 268 . ................................ m/z 57.10 97.57% m/z- > 50 100 150 200 250 300 350 400 450 500 Abundance #78968: Decanedioic acid, bis(2-ethylhexyl) ester 185

57 5000 112 42.20 42.40 42.60 42.80 m/z 70.10 61.43% 83 315

vlz-> 29 I — 50 44 4444 , 200 143 . 213 . 255279 I, A 340 370 397 ................ 100 250150 350 400 450 300 500 Abundance #17577: dl-2-Ethylhexyl chloroformate 57 112 ■ ' i 1 1 1 1 1 1 r' 1 1 1 1 1 KTTTTmT 42.20 42.40 42.60 42.80 5000 83 m/z 71.10 57.20%

■ ‘i” ++H4 149 192 rn/z-> Abundance 50

73 100 150 200 250 300 350 400 #24089: 3-Piperidinone, 1-acetyl-6-methyl- 450 500 P 42.20 42.40 42.60 42.80 112 m/z 55.10 43.49% 43

5000 155

. . | l. j|| . 11 । “i-r-। ITPt:r1I1u" mlz-> 50 100 150 200 250 300 350 400 450 500 42.20 42.40 42.60 42.80

11281.D SCAN020507.M Thu May 16 10:01:01 2002 Page 8

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