NYC-WTC_000024748
Reference document describing Method 509 procedures for laboratory analysis, dated February 14, 1992.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS blank results for sample AE11157, May 2002
Machine-extracted title · confidence 100%Laboratory report showing blank test results for GCMS analysis of sample AE11157 conducted between May 13 and May 16, 2002.
NYC-WTC_000024629–000024639Folder label: “GCMS X 5/13/02 A 5/15/02”
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NYC 9/11 Public Portal Document Llbrary aearen Compound Report
Data File : C:\MSDCHEM\l\DATA\020515\0513LBl.D Vial: 3 Acq On : 15 May 2002 1:48 pm Operator: Nefliu Sample : 05/13 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.46 0.45 ug/1 39015 Naphthal ene-d8 16.53 Hit# Of 5 Tentative -ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 39 3 Benzeneethanamine, N- (pentafluo... 475 C21H26F5NO2Si2 055429-85-1 23 4 Benzoic acid, 2,6-bis[(trimethyl... 370 C16H30O4Si3 003782-85-2 9 Abundance Scan 2107 (15.459 min): 0513LB1.D (-2095) (-) m/ z 73.10 100.00% 73
5000 267 355 IIIn A 15.20 15.40 15.60 15.80 45 179 251 | > 11" ■ । M > TTT T‘‘uI—1/————mu—png m/z 267.00 30.02% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73
- 5000 267 15.20 15.40 15.60 15.80 355 m/ z 3 55.20 27.05% 45 251 28 193 _ ....133149165 ____ mmmm 223 — 307323339 , 96 115 1111" lT" '11 "’ |11 ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73
355 15.20 15.40 15.60 15.80 267 5000 m/z 357.00 16.38%
45 191207223 251 | 323339 ■' I " " I ' r ' ' ' | | | | | " I I I ' I T i I 1-n > | I I i i | n"i I I I T I i I i i TTI—uBI-011r n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115266: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 15.20 15.40 15.60 15.80 m/z 268.90 15.38% 5000 267 44 . .191 117135151 179 209 250 ' I " " lTl 1 IT '' u 11" I TWTTTTTTTTTTTTTTTTTTT '11"' ■ i" " i ‘ " i" ■ ■ i1' n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 15.20 15.40 15.60 15.80
0513LB1.D SCAN020507.M Thu May 16 14:43:12 2002 Page 4
NYC-WTC_000024635
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NYC-WTC_000024635Source: NYC Law Department, mirrored locally
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Laboratory commentary noting no unusual compounds detected in the GCMS scan of sample AE11480 on May 29, 2002.
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NYC-WTC_000045687
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