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GCMS analysis results for sample AE11159, May 2002

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Laboratory report documenting GCMS analysis of sample AE11159 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024681–000024691

Folder label: “GCMS X 5/13/02 A 5/15/02

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NYC 9/11 Public Portal Document uibrary t>earcn compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11159.D Vial: 11 Acq On : 15 May 2002 9:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.46 0.63 ug/1 63792 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 CycfLopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 56 3 Benzeneethanamine, N-[ (pentafluo. . . 475 C21H26F5NO2Si2 055429-85-1 38 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3 37 Abundance Scan 2107 (15.459 min): 11159.D (-2096) (-) m/ z 73.05 100.00% 73

5000 267 355 ' ■ i ■ ■ ' ■ i ' ■ 45 15,20 15,40 15.60 15.80 133 154171 193 249 - "189 ............. 11''' 11 * “ I *'f 11 " ’11' *111 ‘' ‘11'' " I' u' 11 ′′′ 11 '11 *'1 * 339 . 111 “ I'11' 11 "711 ‘ m/z 267.10 40.88% m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundances #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 15.20 15.40 15.60 15.80 m/z 355.10 33.61% 45 191207223 251 | 323339 I 11' " 11711'I'' " I'''* I'1 " I' " 11" ‘'I''1'1'r1 * 111111 u‘1 ‘f “ 1111 ‘ I ” v Tpmp n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

15.20 15.40 15.60 15.80 5000 267 m/z 74.10 10.87% 355

28.14 | 96 115 133149165 , 193 223 251 , 00—01—1— TTPTTTTTTTTTT 307323339 L mfe-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #115266: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 . JJ. 1.. . 15.20 15,40 15.60 15.80 m/ z 268.80 9.80% 5000 267 44 J. , I, 91 117135151 179 209 250 ■ । " I* ' IT’ ■ "i' ' । ■' " । ■ "i 1*pum ."P 11111111 pi 1111111111 " i ‘ ■ i'1" I " " I “ " i " 1 1 i 1 ' 1 1 I 1 1 i ‘ ■ ■ ■ i m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 15.20 15.40 15.60 15.80

11159.D SCAN020507.M Thu May 16 09:54:41 2002 Page 4

NYC-WTC_000024688

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NYC-WTC_000024688Source: NYC Law Department, mirrored locally

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