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GCMS analysis results for sample AE11280, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11280 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024730–000024742

Folder label: “GCMS X 5/13/02 A 5/15/02

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Data File : C:\MSDCHEM\l\DATA\020515\11280.D Vial: 14 Acq On : 16 May 2002 12:39 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.46 0.60 ug/1 59748 Naphthalene-d8 16.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 000541-02-6 370 C10H3005Si5 78 2 Cycl entasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 56 3 3,4- ihydroxybenzyl alcohol,tris... 356 C16H3203Si3 068595-79-9 49 4 Benzeneethanamine, N-[ (pentaf luo. . . 475 C21H26F5NO2Si2 055429-85-1 37 Abundance Scan 2107 (15.459 min): 11280.D (-2096) (-) m/z 73.10 100.00% 73

5000 267 355

45 133 191207223 251 , 15.20 15.40 15.60 15.80 --H — mmmPTT ‘I’" 323 m/ z 2 67.00 40.10% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 15.20 15.40 15.60 15.80 m/z 355.10 37.11% 45 l 191207223 251 । 323339 " i " " i " " I " " i " " I" ■' i1" ' i " " i " " 111T111 ’ " 1" " 11 ”111' " I " " r "' i" 'i" m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

15,20 15.40 15.60 15.80 5000 267 m/ z 356.00 17.03% 355 45 Lau 96 115133149165 , 193 223 251 | T‘B110001—5010000000ugnupT 111" 1IIIFT’ '*i'' 307323339 1 niz->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #27659: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- . A ...... 1, 73 15,20 15,40 15.60 15.80 m/z 267.90 9.95% 5000 267 179 356 45 147 28 1 । 103 131 [ 163 .209 237, । - p " 312 -- - TT—ugo ' "i "'"i 17% q ■ • • • । ' r" ' i ■ "'i"•'r■ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 15.20 15.40 15.60 15.80

11280.D SCAN020507.M Thu May 16 09:59:22 2002 Page 4

NYC-WTC_000024737

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NYC-WTC_000024737Source: NYC Law Department, mirrored locally

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