GCMS analysis results for sample AE08430, May 2002

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Laboratory report listing concentrations of unknown compounds and surrogates in sample AE08430 analyzed on May 16, 2002.

NYC-WTC_000023228–000023237

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document Llbrary aearen compound KeporL

Data File : C:\HPCHEM\l\DATA\MAY0902\8430.D Vial: 10 Acq On : 9 May 2002 11:13 pm Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************* * * Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 1.27 ug/1 107155 Naphthalene-d8 15.83

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo: .ne, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 3,4-Dihydroxyb nzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Benzeneethanamine , N- (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 43 4 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1065 (14.796 min): 8430.D (-) m/z 73.10 100.00% 73

5000 267 355 -- 45 14,40 14,60 14.80 15.00 15.20 -H 1 1111'108125 154 177 193 223 251 — 11W—TmT 323339 | m/z 267.05 32.76% 1' T!**1:—*1+TIuTETrT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14,40 14,60 14,80 15,00 15.20 m/z 355.10 32.17%

’ I’ 1‘ i ■''' i'' ■' i 111 " 11 " ' I'1 ‘' 1 " " I i 191207 11111 TBTTT I’t 2511 323339 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 ■ i ' ' ■ ■ । 1 ■ 171’41’’ 161 1 * 14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 11.69% 5000 179 356 45 147

m/z-> 40 I, ■' r ' " i'1 " i' " ' i " 1' i " ■ ‘ i ■ ■ “ i' 60 4...... 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 312 341 I 11 “ ■1 r ■ " i ■' TTuT Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14,40 14.60 14.80 15.00 15.20 m/z 267.95 9.46%

5000 267 44

m/z—> HH |, 151 179194299 250 |, 1 ‘ I 1 ' ' ' I f ' 1 1 1 1 1 ' I ' ■' " I 1 " ' ’I i । > > । > r i । । । । । । । ' । ' ■ । > I ' । । । i " I" " I " " I PTp'1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15,20

8430.D GCMS0510.M Fri May 10 13:57:32 2002 Page 2

NYC-WTC_000023236

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NYC-WTC_000023236Source: NYC Law Department, mirrored locally

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NYC-WTC_000023353

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