GCMS calibration table for TCLP analysis, May 2002

Machine-extracted title · confidence 90%

Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.

NYC-WTC_000023363–000023371

Folder label: “GCMS X 5/8/02 A 5/9/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document DEaLUii toILpOU KepOIC

Data File C:\HPCHEM\1\DATA\MAY0302\9520.D Vial: 21 Acq On 4 May 2002 9:41 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.79 1.74 ug/1 155579 Naphthalene-d8 15.83

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 47 3 Benzoic cid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 43 4 Benzoic cid, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 38 Abundance Scan 1064 (14,792 min): 9520.D (-) m/z 73.10 100.00% 73

5000 267 355 10 14.40 14.60 14.80 15.00 15.20 45 li 108 133 154170 193 223 251 | 323339 l m/z 267.05 II TI'WWI—ur—u—um 29.36% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 26.51%I 191207 251 |, 323339 1 ■11 ■ T0—mu—mu—ur ' " 111" i'11111" 1'i " i'" i1" ' 11" 11" " I mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 10.10% 5000 179 356 147 209" I " 237 , 1, 312 341 '' i " 1' i'1" i ■ ‘' ' I'1'1 i ‘'1' I'' TrT ' i ■ " i' " ' i' " ‘ i ■1 “ i ■ " ' i1 ‘■ i " " i1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi 73 267 14.40 14.60 14.80 15.00 15.20 m/z 74.10 8.27% 5000

135 47 " i1 ■' " i1 ' | 175 193209 233249 282 । " " I' " ' i " " i1'1' i " “ V " 111'' " I'1 ’’11' i11" i " 11111111111111111111 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14,80 15.00 15.20

9520.D GCMS0501.M Tue May 07 09:38:45 2002 Page 3

NYC-WTC_000023370

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000023370Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS calibration data for TCLP analysis, May 2002 · Box DEP Box 18

NYC-WTC_000023171

Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998