NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\MAR2202\4031.D Vial: 37
Acq On : 24 Mar 2002 5:36 am Operator:
Sample : gc/ms scan 2/25 fb Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.86 1.75 ug/1 290601 Naphthalene-d8 15.90
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91
2 3,4-Dihydro: xybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43
3 Phenethylam/ne, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37
4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4S13 010586-16-0 37
Abundance Scan 1070 (14.864 min): 4031.D (-) ’ m/z 73.00100.00%
73
5000 267 355
...... —
45 154 177 193208223 251 14.60 14.80 15.00i 15.20
I, 89 108125 323 339
TT' T [ ' I r 1TTT ।, i., |'i 11 fT । TT । illIl > । > 293
i TT j"’ ' | T —T m/z 2 6 7.0 0 48.80%
nZ-? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 !
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 / \
5000 i ' 1 1'1
1 14.60 14.80 15.00 15.20
m/z 355.05 44.92%
191 207 251 323 339 2
1‘1‘E731171111111111OIII-ETTTTTTTCTTTTTTTTETTTTTIIT‘TTTTT 111 ■11 ■ i ■1 * • i ■11 • i11 ■11 ■1
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance ' -■ ■ '
73
-......
14.60 14.80 15.00 15.20
267 m/z 356.05
5000 179 17.58%
356
45 147
209 237 312 341
'11'11' 11''' 111' ’ I' ’1 ‘ I''111'' • ’ I'1'11' ’'11'1111'''11'' ‘' I'''' I'11' 11 ‘1' 1111111'111'1
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #74239: Phenethylamine, N-methyl-beta.,3,4-tris(trimethyls /
■ > i • • ■ ■ i ■ ■ ■ ■ i i ■
73 14.60 14.80 15.00 15.20
m/z 268.00 12.97%
5000 355
44
267 294
m/z—?
T’h’
40
— 8 130 147 193
‘1"‘‘‘1‘1111111-111111117177TTTT1111111"T‘11111111——10IUIITUIIIIIT I
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60
/
i 1 1 ' ' i
14.80 15.00 15.20
4031.D GCMS0308.M Tue Mar 26 10:44:44 2002 Page 2
NYC-WTC_000038550
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