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GCMS quantitation results for sample AE04032, March 2002

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Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038552–000038561

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR2202\4032.D Vial: 38 Acq On : 24 Mar 2002 6:35 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 1.23 ug/1 211858 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N- (Trifluoroacetyl) -N,O,O',0' ‘-tetr 553 C22H42F3NO4Si4 000000-00-0 38 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 Abundance Scan 1069 (14.861 min): 4032 D (-) m/z... 73.00 100.00% 3

5000 267 355 --................. 45 I. I ' 1 I 1 1 108 154 ' • I 1 TT i‘ r 1 23,223, +, 2 - 293 323 __ 14.60 14.80 15.00 15.20 m/z 267.00 45.57% m/Z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 - 5000 14.60 14.80 15.00 15.20 m/z 355.05 41.39% 207 , „ 1 323 m/z->50 100__ 150 200 250 300 350 400 450 500 550 Abundance i 73 —..........- 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 14.12%

45 ............. 147 , 193 267 1 538 m/z—> 50 100__ 150__ 200 __ 250 300__ 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-beta.,3,4-tris(trimethyls .......... 4......... 73 14.60 14.80 15.00 15.20 m/z 268.00 12.75% 5000 355

4 147 193 267 294 / TIE ' i ■ ' ' ' i ‘ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

4032.D GCMS0308.M Tue Mar 26 10:45:29 2002 Page 1

NYC-WTC_000038559

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NYC-WTC_000038559Source: NYC Law Department, mirrored locally

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