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GCMS analysis results for sample AE04034, Mar 2002

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Gas chromatography-mass spectrometry analysis report for environmental sample AE04034 dated March 29, 2002.

NYC-WTC_000038571–000038579

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAR2202\4034.D Vial: 40 Acq On : 24 Mar 2002 8:34 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************** ** * *** * * * ******************************** Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.48 ug/1 81235 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzoic agid, 2,4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance Scan 1069 (14.861 min): 4034.D (-) m/z 73.00 100.00% 73 I

5000- 267 355 / 116ETIIIITTT 45 154 193 223 323. 14.60 14.80 15.001 15.20 - 4 r ■' i ‘ ' r T 1 + f rr — ' I ' ’ i ' ' 1 ' i ' ' ' 1 i ' ' 1 1 1 1 ' 1 1 1 1 1 m/z 355.05 44.06% m/z-? 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 5000 267 \ TT-r । 1 1 14.60 14.80 15.00 15.20 m/z 267.00 41.77% 207 || 323 x I Tr m/z—2 _ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 .................... -................... 14.60 14.80 15.00 15.20 5000 - 355 m/z 356.05 15.34% 44 147 193 287294 । i’l 1 । । 1 I । ।

m/z->_.... . 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyijmethylene] 73 14.60 14.80 15.00 15.20 355 m/z 268.00 11.09% 5000

45 I 208 251281 386 458 548 ...... / ■ ■ i ' 1 ' ‘ I........... . f ' I I I "| I ! f ' l ' ' ' ' I ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

4034.D GCMS0308.M Tue Mar 26 10:46:48 2002 Page 1

NYC-WTC_000038578

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NYC-WTC_000038578Source: NYC Law Department, mirrored locally

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