NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration table for TCLP analysis, May 2002
Machine-extracted title · confidence 90%Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09518 analyzed in May 2002.
NYC-WTC_000023345–000023352Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document
Data File C : \HPCHEM\ 1 \DATA\MAYO 3 02\9518.D Vial: 19 Acq On 4 May 2002 7:42 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.80 2.14 ug/1 186535 Naphthalene-d8 15.82
Hit# of 5 'entative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 2 Benzeneethanamine, N-[(pentafluorop 563 3 Benzoic acid, 2-[(trimethylsilyl)ox 282 4 3,4-Dihydrpxybenzyl alcohol,tris(tr 356 C10H30O5S15 000541-02-6 C24H34F5NO3Si3 055429-13-5 C13H2203Si2 C16H3203Si3 003789-85-3 43 068595-79-9 43 1 Abundance Scan 1065 (14.797 min): 9518.D (-) m/z 73.10 100.00% 73
5000 267 355 -
45 14.40 14.60 14.80 15.00 15.20 - 108 r i 154 193 223 1‘*14-1" i- i i Hi 323 m/z 267.05 34.94% TBit ■ ■ i" ■ 1 ■ । 1 1 1 1 i 1 ' 1 1 । ■ 1 1 ■ i ' ‘ mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 1 14.40 14.60 14.80 15.00 15.20 m/z 355.10 34.19% 207 „ 1 323, TTTk mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 14 40 14.60 14.80 15.00 15.20 5000 m/z 356.10 12.08%
45 . I . ..... 1 1 i ' ' ■ ■ i ■ ■ 1 ' i 1 1 208 251 281 TFr I.... " 386 458 548 ■n/z—> 50 100 150 200 ' 250 300 350 400 450 500 550 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi 73 267 14.40 14,60 14.80 15.00 15.20 m/z 268.05 9.29%
5000
m/z—> 47 ' 11 ■ ' ... 135.193,233 .....-..... ............... ■ ■ i ■ ' ■ ' i ' ' 1 ■ i ' 1 ' ' 1 ' 1 ■ ' i ' ‘ ' i 1 ' ' ■ i ' 1 ■ ' i ' ' ' ' i ' ' ■ ■ i ■ ■ 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9518.D GCMS0501.M Tue May 07 09:38:15 2002 Page 2
NYC-WTC_000023351
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