GC/MS calibration table, sample AE08934, April 2002

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Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.

NYC-WTC_000043726–000043734

Folder label: “GCMS X 4/24/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2302\8934.D Vial: 14 Acq On : 24 Apr 2002 3:05 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:31 2002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE or) Title : 209 625/TCLP calibration table Last Update Response via DataAcq Meth : : : Wed Apr 17 11:48:30 2002 Initial Calibration GCMS0412 < y*' Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 547297 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 2019801 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.15 164 1138768 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.58 188 1655537 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 1079624 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 685108 20.00 ug/1 -0.05

System Monitoring Compounds 2 8) TCMX 23.28 209 34739 6.09 ug/L -0.05 Spiked Amount 10.000 Recovery = 60.90% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.90 128 314 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.42 165 186 N.D. 25) Diethylphthalate 22.62 149 807 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration 8934.D GCMS0412.M Wed Apr 24 08:32:22 2002 Page 1

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GCMS calibration table for TCLP analysis, April 2002 · Box DEP Box 25

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Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.

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