GCMS calibration data for TCLP analysis, May 2002

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Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

NYC-WTC_000023171–000023178

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7 Data File C:\HPCHEM\l\DATA\MAY0302\9576.D Vial: 49 •/ Acq On 5 May 2002 3:03 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:55 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.19 152 540710 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1988944 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.13 164 1079371 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1507488 40.00 ug/1 -0.01 38) Chrysene-dl2 33.64 240 975239 40.00 ug/1 -0.02 44) Perylene-dl2 37.87 264 639451 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.27 209 20094 3.82 ug/L -0.02 Spiked Amount 10.000 Recovery = 38.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 329 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 1657 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 9) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.58 178 372 N.D. (#) = qualifier out of range (m) = manual integration 9576.D GCMS0501.M Tue May 07 14:56:27 2002 Page 1

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GCMS calibration data for TCLP analysis, May 2002 · Box DEP Box 18

NYC-WTC_000023148

Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

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