NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration table for TCLP analysis, May 2002
Machine-extracted title · confidence 90%Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09578 analyzed in May 2002.
NYC-WTC_000023327–000023334Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0302\9578.D Vial: 51 Acq On 5 May 2002 5:01 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Miso Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.79 4.22 ug/1 367038 Naphthalene-d8 15.83
Hit# of 5 'entative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 3 Benzoic/acid, 2,4-bis (trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 Benzoic acid, 4-[(trimethylsilyl)ox 282 C13H2203Si2 - 002078-13-9 37 Abundance ' Scan 1064 (14.794 min): 9578.D (-) m/ z 73.10 100.00%| 73
5000 267 355 ,............. 45 14,40 14.60 14.80 15.00 15.20 — 125 154 193 223 293 323, l.......... m/z 267.05 32.02% mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14,40 14.60 14.80 15.00 15.20 m/z 355.10 29.77%! , , ——m/m/ 1-1d***/n 207 . 323 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355
14,40 14.60 14,80 15.00 15.20 5000 m/z 356.10 10.93%|
45 | | 208 251 281 1 386 458 548 ‘ ' i ' ' 1 ' i 1 ' ' ■ i ' ' ' ■ i ' ■ ■ ( ' i ■ ■ mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy}-, trimet 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 8.35%
5000 355 l 45
[ 133 193 223 281। m!z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9578.D GCMS0501.M Tue May 07 15:02:01 2002 Page 2
NYC-WTC_000023333
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NYC-WTC_000023333Source: NYC Law Department, mirrored locally
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Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
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Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
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Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09518 analyzed in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044621
Calibration scan report for EPA Method 625 showing retention times and deviations for deuterated standards on April 25 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
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Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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