GCMS analysis results, sample AE09393, May 8, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\MAY0102\9393.D Vial: 11 Acq On 1 May 2002 5:16 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.81 1.02 ug/1 93730 Naphthalene-d8 15.84 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(8 2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 47 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 40 4 N-(Trifluor/>acetyl)-N,O,O',0' '-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 1066 (14.809 min): 9393.D (-) m/z 73.10 100.00% 73

5000 267 355 — - 45 14.40 14.60 14.80 15.00 15.20 108 154 191 223 323, i - ' 1’*** r ■' ■ 1" ** । tr । m/z 355.10 31.85% m/z-->____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 1 ' 1 1 1 1 1 Tl I 14.40 14.60 14.80 15.00 15.20 m/z 267.05 31.59% 207 323, ■ 1 । 1 rn/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 ......................). 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 10.37%

45 208 251 281 386 458 548 r ' i ■ ' 1 ' i 1 TII—B———n——-TT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ___________ 73 14.40 14.60 14.80 15.00 15.20 m/z 74.10 8.32% 5000- 355 44

m/z-> L 147 193 267294 | 1 'I 1 ' 1ti । • । 1 | । > i i । i i । । [ r i i i' । i । i । । । । I I | I i । । । । । I I | i" | | | । — 50 100 150 200 250 300 350 400 450 500 550 ..... 11 14.40 14.60 14.80 15.00 15.20

9393.D GCMS0501.M Thu May 02 12:02:40 2002 Page 3

NYC-WTC_000043088