GCMS analysis results, sample AE09393, May 8, 2002

NYC 9/11 Public Portal Document

Data File C: \HPCHEM\ 1 \DATA\MAY 0102\9393.D Vial: 11 Acq On 1 May 2002 5:16 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.96 1.27 ug/1 116886 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 10 4 2H-1,4-Benz/odiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 Abundance 7 Scan 1410 (17.961 min): 9393.D (-) m/ z 73.10 100.00% 73

5000- 341 147 429 45’ , 17.60 17.80 18.00 18.20 ,1 1’11 I 117 179. 207 251 311 L 1............... k I i | r i > i । TH "I T j : < ( f | < i / i | I T f i ] i i i r j < i I I | I I i i । i i i I | i i I i | i 1 i i । i i r > | 1 i i I j I i i l | T i i i । i t t i । i i i i । i i I I | I ri I | I m/z 341.00 30.33% m/z-> 40 60 80 100120140160180200220240260280300 320340360380400420 Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341

429 ................... )...................... 5000 ' i 1 1 1 ’ i ■ 1 1 ' i 1 1 ■ ■ i ■ ■ ' 1 1 1 17.60 17.80 18.00 18.20 m/Z 147.15 14.67% 147 [ 207 267 311 [ 117 ।"111" " i"" i UOnu——0———mu0—mmg0u0mag m/z~> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 ■ i 1 1 1 ■ i * ' ‘ 1 1 1 1 1 ''"I 1 147 17.60 17.80 18.00 18.20 267 m/z 429.05 10.87% 5000 355 429 45 207

r " 11" " r " ‘ i I........ ............ | I I I I | | I r i | i i i f | I I I I | I I i r | I i i i | I I I I | i I ( i I ' i ‘"1 r " 11" " i" 11 r m/z~> Abundance 40 60 80 100120140160180200220240260280300320340360380400420 #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- II n ■R 73 17.60 17.80 18.00 18.20 m/z 342.00 10.39% 239 5000 342

45 133, 179 211 314 i 11111" i ■ ■ ■■ ।11" i i11111111" " 11111111 i TT IT m/z-> 40 60 80 100120140160180200220240260280300320 340 360 380 400 420 17.60 17.80 18.00 18.20

9393.D GCMS0501.M Thu May 02 12:02:41 2002 Page 4

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