Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
NYC-WTC_000043146–000043160Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclohexasiloxane, dodecamethy Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
17.96 3.23 ug/1 248217 Naphthalene-d8 15.84
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
I Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 47 2 4-Amino-5-imidazole carboxamide, tr 342 C13H30N4OSi3 000000-00-0 32 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 4 Silane, [1,2,3/benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance / Scan 1410(17.959 min): 9398.D (-) m/ z 73.10 100.00% 73
5000 341 i | T i ii । i i 1 i pi I 1 i i Ii | i
147 429 17.60 17.80 18.00 18.20 45
m/z-> 207 179 TITh 1171 251 I..................................... .............311 . ..................... T i I | i i I r | i i i i | i i i ■ । i Ii Ii Ii ।I ।I ■ ।I 1i ।I >i Ii Ii 1i I| I। i i । | i i i i | । । । i | । i i t | i ■ i i | > i i ■ | i i i । j । । । । | । । । i | i i i > | i i i i | i i i i | i "i“ 40 60 80 1001201401601802002202'40260280300320340360380400420 hi m/z 341.00 26.00% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 ..................).................... 5000 I ' |— I I I ’ l— | I l l I | I I I k T I I I | I
17.60 17.80 18.00 18.20 m/z 147.05 12.94% 147 117 [ 207 267 311 [ ‘" r'" i" " r 1" i" " r ■" i1'" i" " i " " i11" i" " i" " ir ‘" r111 r 111 r1" P "' r '" i" " r 11 ‘' i' m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48317: 4-Amino-5-imidazole carboxamide, tris(trimethylsily 73 1 1 i ■ ■ ■ ■ i 1 327 17.60 17.80 18.00 18.20 5000 m/z 342.00 9.45% 237 45
/z—> ..147 172 I'1'11 ■ H ' I"111 21? 44 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 73 #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethy lsiloxy)t Ti J 1’I i ‘ ■ 1 ' 1 1 17.60 17.80 1 8.00 18.20 m/z 429.05 8.97% 147 5000 267 355 429 45 207 L 1115 r. 11 > । > । ... I.. 111111 TTTTTTTTTTTTTTTTT /z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.60 17.80 18.00 18.20
9398.D GCMS0501.M Thu May 02 12:04:39 2002 Page 6
NYC-WTC_000043156
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045223
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10432 conducted on May 20, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044723
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023148
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
Filed in the same folder
NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
Filed in the same folder
NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
Filed in the same folder
NYC-WTC_000043046
Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
Filed in the same folder
NYC-WTC_000043050
Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
Filed in the same folder