GCMS calibration table, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAY0102\9398.D Vial: 16 Acq On : 1 May 2002 9:54 pm Operator: Sample : gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 lH-Inden-5-ol, 2,3-dihydro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

16.42 0.67 ug/1 51374 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1H-Tnden-5-ol, 2,3-dihydro- 134 C9H10O 001470-94-6 90 2 Benzaldehyde , 2, 4-dimethyl” 134 C9H10O 015764-16-6 86 3 Be n z a l dehyde, ethyl - 134 C9H10O 053951-50-1 86 4 Benzaldehyde, 3,4-dimethyl- 134 C9H10O 005973-71-7 86 Abundance Scan 1242 (16.419 min): 9398.D (-) m/z 133.10 100.00% 133

105 5000 77 39 51 91 ' | I I I k t 1" I |' l k1 I | I-! l [ । i

_____ J , 45 I ii - | I I I I | I 1 ! I j1! — 63 11 Ii ii I । ।__ i _i 1....... 16.00 16.20 16.40 16.60 16.80 m/z 134.10 83.38% ' [ ( 1 1 1 1 ( 1 ' ' I 1 1 ' 1 I I I I ' I I ' 1 I I I 'V ' I I ‘ I ' I I I I I I I ■ 1 i ■ ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6183:1 H-lnden-5-ol, 2,3-dihydro- 133

I । । । i 11 i I T] । । 1 i [ i ki । । > r 5000 16.00 16.20 16.40 16.60 16.80 77 105 m/z 105.15 58.14% 63 1 I ' ' 1 1 i ' ' ' 1 i 1 Il 7 r-] i l i । i i i । । । r i i । i i n । । i~i i [ T 89... 1 T-TTTTPPTTTT 117 1 ' I ' 1 mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6179: Benzaldehyde, 2,4-dimethyl- 133 ....... 1........ 105 16.00 16.20 16.40 16.60 16.80 5000 m/z 77.10 28.04%

77 27 51

m/z—> \ 20 I 30 40 1-p 50 r 60 . 80.... 70 90 100 1 122 41—— i ■ > i * ■ 110 120 130 140 Abundance #6154: Benzaldehyde, ethyl- | I I I 1 [“I I I T| I f [1 [ I I I I | I I

133 16.00 16.20 16.40 16.60 16.80 m/z 79.10 20.91% 105 5000

77 51 119 ........ I ' ( ■ ■ • I I ' I ' ' 189.... 1I !. j.. I......... I ! I I I I I I I I I I i । । । । i n । i n i | > ■ ■ i ■ ■ ।_ r । 1l i i । i > i i । i r m/z-> 20 30 40 50 60 70 80 90 100> 110 120 130 140 16.00 16.20 16.40 16.60 16.80

9398 .D GCMS0501.M Thu May 02 12:04:38 2002 Page 5

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