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GCMS instrument log for sample AE09676, May 2002

Machine-extracted title · confidence 95%

Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.

NYC-WTC_000023789–000023810

Folder label: “GCMS X 5/9/02 A 5/20/02

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Scanned page image, NYC-WTC_000023800
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Benzaldehyde, 3,4-dimethyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

16.36 0.87 ug/1 61538 Naphthalene-d8 15.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzaldehyde, 3,4-dimethyl- 134 C9H10O 005973-71-7 Q. 2 Benzaldehyde, 2,4-dimethyl- 134 C9H10O 015764-16-6 87 3 Benzaldehyde, 4-ethyl- 134 C9H10O 004748-78-1 86 4 1H-Inden-I-ol, 2,3-dihydro- 134 C9H10O 006351-10-6 78 Abundance Scan 1236 (16.363 min): 9676.D (-) m/z 133.10 100-. 00% 133

105 5000 77 39 51 91 I 1 1 1 1 i TT 63 16.00 16.20 16.40 16.60 16.80

m/z-> 20 -PP-II 30 40 50 60 70 90 80 100 । 'J'. u 110 120....130 140 m/Z 134.10 79.06% Abundance #6182: Benzaldehyde, 3,4-dimethyl- 133

105 .................. /,).............. 5000- 16.00 16.20 16.40 16.60 16.80 77 m/z 105.15 58.66% 51 .......... I....... Il , , ' ' ।92~ ' ' i Hi|, +119... 1 i 1 ' ' ' i ' 1 ‘ 1 i ' 1 ■ ' i ' ' ‘ 1 i ' ' ' ' i ' ' ' ■ i ' 1 i

m/z—> 20 30 40 50 60 70 90 80 100 110 120 130 140 Abundance #6179: Benzaldehyde, 2,4-dimethyl- 1:3 - 105 16.00 16.20 16.40 16.60 16.80 5000 m/z 77.10 28.11%

77 27 51 | JL ■ i ■ ■ ■ ■ i ■ ■ ■ » i ■ ■ ■ ' i ■ > 1 ■ । 1 • ■ ■ । » • ■ ■ । ■ ■ . । । । 122 1 1 1 1 1 r ' i 1 i

m/z-> 20 30 40 50 60 70 80 90 100110 120 130 140 Abundance #6187: Benzaldehyde, 4-ethyl- ,*.......... , 133 16.00 16.20 16.40 16.60 16.80 m/z 39.00 19.11% 91 5000 105

77 119 .... । । . Il . ....... । ....... ।। । , ।. , , , ’II, —i■■■ ■। ■1 ■ । ■ 1 AMA— ' 1 I 1 1 1 1 I 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 16.00 16.20 16.40 16.60 16.80

9676.D GCMS0520.M Tue May 21 11:39:17 2002 Page 5

NYC-WTC_000023800

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NYC-WTC_000023800Source: NYC Law Department, mirrored locally

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