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GCMS analysis results for sample AE11602, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013943–000013967

Folder label: “GCMS X 5/24/02 A 5/28/02

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Scanned page image, NYC-WTC_000013950
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11602.D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2**

Quant Method : C»\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) ** Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Benzene, 1,2-dimethyl- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 8.82 0.52 ug/1 33348 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1,2-dimethyl- 106 C8H10 000095-47-6/91 2 Benzene, 1,3-dimethyl- 106 C8H10 000108-38-3 91 3 p-Xylene 106 C8H10 000106-42- 91 ) 4 1,3-Cyclopentadiene, 5-(1-methyleth 106 C8H10 002175-91- 83/ Abundance Scan 412 (8.820 min): 11602.D (-) m/z 91.10 100.0 91

106 5000

39 51 65 77 8.40 8.60 8.80 9.66 9.20 11 m 1111111111111111 [ 1111 i i-rf-lli(|iiri [ill vi i n u nibl|ii | hsuuipsha —pmp m/z 106.05 50.73% miz-> 20 25 3035404550 55 6065 70 75 80859095 100 105 110 115 Abundance #63706: Benzene, 1,2-dimethyl- SI

106 A 5000 8.40 8.60 8.80 9.00 9.20

51 m/z 105.15 20.19% 27 77 • i * • • • । > t *’•>i*•*■i1 * * *i•>•*।■i••" ।* •»। > •«> । TI‘11 kmmm 4pm niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 Abundance #63696: Benzene, 1,3-dimethyl- 91

106 8.40 8.60 8.80 9.00 9.20 5000 m/z 51.05 12.73% __

51 TTTTTTTTTTTTImp 1111 rrr i! t —pmpn 65 77 miz-> 20 25 3035404550556065 70 75 80859095 100105110115 Abundance #63699: p-Xylene SI 8.40 8.60 8.80 9.00 9.20 m/z 39.00 12.10% 106 5000

TmTTTTHm 51 6577 n/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115 8,40 8.60 9.20

11602.D GCMS0520.M Fri May 24 08:33:07 2002 Page 3

NYC-WTC_000013950

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NYC-WTC_000013950Source: NYC Law Department, mirrored locally

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