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GCMS calibration table for TCLP analysis, Nov 2 2001

Machine-extracted title · confidence 100%

Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.

NYC-WTC_000067979–000067989

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\LB.D Vial: 2 Acq On : 31 Oct 2001 5:05 pm Operator: 209 GALOS Sample : 10/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Benzene-1,2,3,4-d4-, 5,6-dichl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 88614 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 ntative ID MW MolForm CAS# Qual 1 Benzene-3^,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 56 2 1,4-DichZorobenzene-d4 150 C6C12D4 003855-82-1 47 3 1,2,5-^ithiepane 152 C4H8S3 006576-93-8 10 4 Benza^ehyde, 2-hydroxy-5-methoxy- 152 C8H8O3 000672-13-9 9 Abundance/ Scan 711 (11.569 min): LB.D (-) m/z 149.90 100.00% 1ii0

5000 115

52 78 n 11.20 11.40 11.60 11,80 -TTyT-TT-i-pTMrp-r-TTq-i-^^ m/z 151.90 69.12% n&-> 30 40 50 60 75 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3.4-d4-. 5,6-dichloro- 1!»

115 5000- 52 78 I I > I I I I . . I Tl I t I , , . , , 11.20 11.40 11.60 11.80 m/z 115.00 38.35% 87 nfe-> 35 I "30 " '40 " » ” '00 1 ■ I • < I • I • " ■ I • 70 80 90 100 110 12P 130 A 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 DiO

11.^' '1D40 IDSO 'ipao' " ' ‘ 50)0 115 m/z 78705 16.93% 52 78

35 TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10068:1.2,5-Trithi8pane D2 m/z 52.00 14.38% 5000 60 87 (I 45 78 106 I ■ 1 • ■ ■ • I • • I ■ I • 4^ .................. Ti&-> 30 40 50 60 '' 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

LB.D NP103001.M Fri Nov 02 17:17:26 2001 Page 4

NYC-WTC_000067988

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NYC-WTC_000067988Source: NYC Law Department, mirrored locally

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